Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A
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These tests are often run as a aetm test to ensure each batch of stainless steel is properly prepared. Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation.
For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions. The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels.
ASTM A Intergranular Corrosion Testing and Analysis
Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. Because it can be run quickly for screening, we often run this test first. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations atm to use.
Like what you saw? Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed.
Share on Tumblr Print. Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself. Duplicate samples from both sides of a sheet sample are evaluated to determine if prcatice results in intergranular attack. Intergranular corrosion shows up as the dark black lines around the a2262 boundaries.
Please refer to the specification for more details. Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys. Based on your materials, application, and requirements, the other 4 methods provide specific focuses. It is typically used for stainless alloys v as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries. Atsm specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels.
In everyday applications, corrosion varies by materials and solutions. The inch-pound equivalents are in parentheses and may be approximate. Contact us now for pricing or a quote! Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application. Please specify the maximum allowable corrosion rate and q262 available data on the sensitizing heat treatment performed. These tests do not provide a basis for predicting resistance to forms of corrosion other than intergranular, such as general corrosion, pitting, or stress-corrosion cracking.
The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades. The first and fastest step is the Practife A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion.
These practices include five intergranular corrosion tests, namely: The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.
A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for use. This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively.
Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack.
From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment. Practice B, also known as the Streicher test, uses weight loss analysis to provide a quantitative measure of the materials performance. Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.